The synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressure 328605004

The synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressure

[ De synthese van [2-13C]2-nitropropaan bij kamertemperatuur en atmosferische druk ]

Jacquemijns M, Zomer G

15 p in English 1990

RIVM Rapport 328605004

Toon Nederlands

English Abstract
In this report the synthesis of [2-13C]2-nitropropane at room temperature is described. [2-13C]Acetone was converted into the oxime with hydroxy hydrochloridelamine and sodium carbonate. Treatment with hypobromic acid resulted in 2-13C]2-bromo-2-nitropropane. Hydrogenation with sodium borohydride gave [2-13C]2-nitropropane in 14,3% overall yield.

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_{( 1990-03-31 )}